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51.
Imaging techniques based on neutron beams are rapidly developing and have become versatile non-destructive analyzing tools in many research fields. Due to their intrinsic properties, neutrons differ strongly from electrons, protons or X-rays in terms of their interaction with matter: they penetrate deeply into most common metallic materials while they have a high sensitivity to light elements such as hydrogen, hydrogenous substances, or lithium. This makes neutrons perfectly suited probes for research on materials that are used for energy storage and conversion, e.g., batteries, hydrogen storage, fuel cells, etc. Moreover, their wave properties can be exploited to perform diffraction, phase-contrast and dark-field imaging experiments. Their magnetic moment allows for resolving magnetic properties in bulk samples. This review will focus on recent applications of neutron imaging techniques in both materials research and fundamental science illustrated by examples selected from different areas.  相似文献   
52.
臭氧氧化-循环喷淋法处理钨钼选矿废水   总被引:4,自引:0,他引:4  
采用臭氧氧化-循环喷淋法去除钨钼选矿废水中COD,研究了pH值、臭氧流量、循环频率对COD去除效果的影响。结果表明: 废水COD去除率随pH值、臭氧流量、循环频率增大而增加,在pH值为10、臭氧流量3.0 L/min、循环频率4.0次/min条件下,氧化120 min后废水COD含量由131 mg/L降至11.5 mg/L,COD去除率达91.2%,满足《污水综合排放标准》(GB 8978-1996)一级标准。与O2、NaClO处理废水COD的对比试验结果表明,循环喷淋法结合O3表现出较好的COD去除效果。  相似文献   
53.
Ca0.9La0.067TiO3 (abbreviated as CLT) ceramics doped with different amount of Al2O3 were prepared via the solid state reaction method. The anti-reduction mechanism of Ti4+ in CLT ceramics was carefully investigated. X-ray diffraction (XRD) was used to analyze the phase composition and lattice structure. Meanwhile, the Rietveld method was taken to calculate the lattice parameters. X-ray photoelectron spectroscopy (XPS) was employed to study the valence variation of Ti ions in CLT ceramics without and with Al2O3. The results showed that Al3+ substituted for Ti4+ to form solid solution and the solid solubility limit of Al3+ is near 1.11 mol%. Furthermore, the reduction of Ti4+ in CLT ceramics was restrained by acceptor doping process and the Q × f values of CLT ceramics were improved significantly. The CLT ceramic doped with 1.11 mol% Al2O3 exhibited good microwave dielectric properties: εr = 141, Q × f = 6848 GHz, τf = 576 ppm/°C.  相似文献   
54.
Qualitative analysis of aeromagnetic data of part of Nasarawa State had been carried out with the aim of delineating mineral potential zone. The study area is bounded by Longitude 8.0°E – 9.0°E and Latitude 8.0°N – 9.5°N with an estimated total area of 18,150?km2. Different filters were used to enhance the short wavelength anomalies which could give preliminary information about the magnetic minerals present in the study area. The total magnetic intensity map shows variation of both highs and lows magnetic signature ranges from ?51.2?nT to 110.4?nT after the removal of IGRF value of 33,000?nT; the highs which is basement dominates the north-eastern and north-western part of the study area which corresponds to Akwanga, Wamba and Nasarawa Eggon; these are areas with promising solid minerals of economic potentials like, gold at Wamba; Tin, Columbite and Tantalite at Akwanga while Granite rocks with possible radioactive elements are in abundance at Nasarawa Eggon. The low magnetic values on the other hand, which is made up of sediment deposition also dominates the southern part of the study area, this area corresponds to Lafia, Doma and Keana; Lafia and Doma host some industrial minerals like Clay, glass Sands and the Salt Brines at Keana. The major high magnetic signature trends east-west. The greenish part of the study area indicates alluvium deposition. The filters used are vertical derivatives, downward continuation and analytic signal. The first and second vertical derivatives; shows structures like lineament that could be the host to minerals present in the study area and it trends NE-SW. The downward continued at the depth of 50?m and 100?m shows the veins where magnetic minerals most especially gold are known to settle along igneous and metamorphic rocks. The analytic signal map shows that magnetic amplitude highs could be found at the northern end with most lineaments delineated also conform to other filter used. The tilt derivative map enhances short wavelength anomalies which could be used to mapped shallow basement structures and mineral exploration targets. The results of these filters agreed largely and since most magnetic minerals are structural controls, it is expected that those lineaments identified, most especially at the northern part, could play host to those minerals aforementioned.  相似文献   
55.
The research analyses decisions as evaluative outcomes regarding project value. The UK-French Hinkley Point C Nuclear Power Station provides the case study. Value is traditionally assessed as inputs and outputs. Here, value is conceptualized as a co-created value proposition at the front-end with implications for realization post-completion. Service-dominant logic (SDL) provides the theoretical lens and contributes to a methodological approach for examining projects. Decision-making outcomes provide the evidence from a range of data sources, including reports and commentaries. The methods are interpretative. The findings show that decision-making extends beyond the time-cost-quality/scope dimensions. The long-term issues regarding value realized are often overlooked. Stakeholders and individual actors have mainly focused upon managing political and financial risks, especially time and cost. The research poses challenges to project management analysis, SDL and research design in assessing evidence. Addressing these issues facilitates a knowledge contribution to SDL theorization and the field of project management.  相似文献   
56.
《Advanced Powder Technology》2020,31(11):4552-4562
Magnetic nanoferrites (MFe2O4, M = Co, Ni) were successfully synthesised through microwave-hydrothermal route, characterised and used for adsorption of Eriochrome Black T (EBT) and Bromophenol Blue (BRB) dyes from their aqueous solution. The powder XRD patterns confirmed the formation of cubic spinel structure for both the ferrites. Under identical conditions, the adsorption efficiency of CoFe2O4 was found relatively higher than the corresponding NiFe2O4. Further characterisations revealed that CoFe2O4 sample was nearly spherical in size (8–9 nm) with narrow size distribution. The sample showed superparamagnetic behaviour with saturation magnetization (Ms) value (66.4 emu/g). BET surface area calculated for the synthesized cobalt ferrite as 70.9 m2/g. Batch adsorption experiments as a function of initial dye concentration, pH, contact time and adsorbent dose showed the adsorption of dyes depends on pH. Equilibrium adsorption data were well explained by both Langmuir and Freundlich isotherm models. The maximum monolayer adsorption capacities (Qo) were found to be 82.6 and 25.6 mg/g for EBT and BRB dyes, respectively. Kinetics of the adsorption was best described by pseudo-second-order model. Various thermodynamic parameters such as ΔG, ΔH and ΔS derived from adsorption data over the temperature range 20–50 °C, accounted for a favourable, spontaneous, endothermic physisorption process. The materials showed potential for repeated use without significant decrease in adsorption capacity after proper regeneration.  相似文献   
57.
In the present research, the effects of continuous ultrasound treatment (100 W, 30 kHz; 0%, 30%, 60% and 90% amplitudes, 15 min) and fermentation process (37°C, 24 h) on the growth of Lactobacillus plantarum LP3 and LU5 strains and bioactive properties (peptide content, α-amylase and α-glucosidase inhibition, anticancer and antioxidant activities and exopolysaccharide content) of goat milk were investigated. According to our results, the ultrasonication of milk up to 60% amplitude promoted the growth of Lactobacillus strains and enhanced the bioactive properties compared with control during fermentation, while, the ultrasonication at 90% amplitude had negative effects on the mentioned parameters. Exopolysaccharide content, α-amylase inhibition, α-glucosidase inhibition, antioxidant activity and anticancer activity of treated samples at 60% amplitude at the end of fermentation in comparison to its beginning were increased 18.09, 12.79, 12.44, 9.4 and 1.92 folds, respectively. Also, the increase of assayed characteristics was found strain-dependent, so that L. plantarum LP3 was more effective than LU5 strain.  相似文献   
58.
59.
Public-private partnerships (PPPs) are predominantly executed through the use of formal contracts which define the relationship between a public agency and private supplier. As such, a PPP is not a generic contract between buyer and supplier but rather a specific contractual arrangement between a public buyer and private supplier. The contract captures the responsibilities of each party in achieving a specific set of performance objectives. Given budgetary pressures faced by public agencies, there is an increasing need for suppliers to make investments which could reduce future-year costs of meeting contract performance objectives. This research addresses two overarching questions specific to the issue of private, supplier-side investment. First, “how does public agency and private supplier perception of risk influence contract duration?” and second, “how does contract duration influence private investment?” To answer these questions, structured interviews were conducted with those in public agencies and private, supplier firms actively engaged in PPPs. Factors suspected to contribute to the risk position of public and private actors were evaluated. Additionally, linkages between public buyer-private supplier risk position, contract duration and private, supplier-side investment were addressed. Outcomes suggest properly structured long-term contracts may: 1) provide the risk mitigation mechanisms needed for both public and private actors, and 2) facilitate private, supplier-side investment.  相似文献   
60.
以废弃的流化催化裂化催化剂(简称SFCC)为载体、β-环糊精为金属络合剂、硝酸镍为镍源,采用湿法浸渍法制备β-环糊精修饰的Ni/SFCC催化剂(简称Ni/SFCC-CD催化剂),考察其对C9石油树脂的催化加氢性能。通过BET比表面积测试、H2程序升温还原、X射线光电子能谱等手段对催化剂的物相结构进行表征,研究β-环糊精的作用机理及其对催化剂加氢性能的影响。研究结果表明:在反应温度为260 ℃、反应压力为7 MPa、反应时间为2.0 h的最优条件下,采用Ni/SFCC-CD催化C9石油树脂加氢,可制得溴值为1.45 gBr/(100 g)、色号(加纳德)小于1的水白色氢化C9石油树脂,催化剂循环使用4次后仍保持良好活性;β-环糊精的作用机理是:β-环糊精与硝酸镍产生络合作用,抑制硝酸镍的分解、控制NiO的结晶过程和增强活性组分Ni与载体之间的相互作用力,从而提高了Ni/SFCC-CD的催化活性和稳定性。  相似文献   
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